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酸棗仁湯エキス/HILIC
酸棗仁湯エキス/HILIC
【ODS】

漢方方剤名 酸棗仁湯 (さんそうにんとう)
構成生薬 酸棗仁 15, 茯苓 4, 川芎 3, 知母 3, 甘草 1
原典 金匱要略
化合物名 Mangiferin 7-glycoside,Zizyphusine,Timosaponin E,Apioliquiritin,Liquiritin,Timosaponin B,Licorice-saponin G2,Glycyrrhizin,Sucrose,Proline
分析条件  
備考  

【 EXP017001 】
Peak No.123456789101112131415
Compound nameTimosaponin E  Sucrose Timosaponin B Glycyrrhizin  Proline    
tR(min)4.25.289.5210.4112.0112.9414.9415.3216.2518.1518.6519.4319.8423.3124.07
UV/Vis max (nm) 1       249       
UV/Vis max (nm) 2               
UV/Vis max (nm) 3               
UV/Vis max (nm) 4               
UV/Vis max (nm) 5               
HR-MS 1 (base peak, m/z)423.09183268.10379244.09265360.14986418.17045903.49374286.14363522.20262342.17002176.09156116.07039160.09665160.09663122.92426254.16106
HR-MS 1 intensity100100100100100100100100100100100100100100100
HR-MS 2 (2nd)424.09521269.10709360.14976404.15482360.14991938.53082522.2025840.43708343.17335177.09492278.12336161.09999176.10276206.88573255.16441
HR-MS 2 intensity20.2110.945.819.5759.0568.7627.3323.4221.617.5711.527.4978.3895.411.66
HR-MS 3 (3rd)342.13932423.09174112.05029325.1128419.17381360.14979287.14697523.20594132.10177133.0605670.06495319.18634138.05475290.84708122.92432
HR-MS 3 intensity13.847.0237.2114.1919.4658.2918.1118.6811.936.539.95.3128.7289.539.02
HR-MS2 for base peak, 1261.00656  145.06287272.09958255.22229 162.9462253.08185      
HR-MS2 for base peak, 2273.13501  163.02287 273.17389 288.9985265.06094      
HR-MS2 for base peak, 3285.14667  179.92407 285.23236 324.9248267.18771      
HR-MS2 for base peak, 4303.06577  198.177 381.28076 342.27734279.03711      
HR-MS2 for base peak, 5327.06348  258.82507 399.25165 342.97888282.14667      
HR-MS2 for base peak, 6356.95007  288.92749 417.26038 450.86707285.11017      
HR-MS2 for base peak, 7369.02509  306.87332 435.12616 468.67291297.04861      
HR-MS2 for base peak, 8386.98425  324.91754 561.19232 486.64191299.0419      
HR-MS2 for base peak, 9405.01178  341.99417 579.24774 503.91681311.07327      
HR-MS2 for base peak, 10   342.8558 741.1889 504.64471313.19171      
HR-MS2 for 2nd MS, 1274.1745 162.99536272.11029127.16917676.49554 320.16452265.02847      
HR-MS2 for 2nd MS, 2303.06055 180.10837 145.05441  431.25732266.05768      
HR-MS2 for 2nd MS, 3304.0358 198.10117 163.01019  470.29993280.09723      
HR-MS2 for 2nd MS, 4327.21814 259.00305 258.89185  488.31854297.09647      
HR-MS2 for 2nd MS, 5328.00421 288.37906 288.86719  592.18225298.08069      
HR-MS2 for 2nd MS, 6352.00052 289.10632 306.93445   299.19244      
HR-MS2 for 2nd MS, 7357.95068 307.01129 324.28192   300.06274      
HR-MS2 for 2nd MS, 8370.04407 324.89859 324.88757   311.10046      
HR-MS2 for 2nd MS, 9388.02618 341.74265 342.01913   312.10004      
HR-MS2 for 2nd MS, 10406.07285 342.73972 342.8941   314.15417