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防風通聖散エキス/HILIC
防風通聖散エキス/HILIC
【ODS】

漢方方剤名 防風通聖散 (ぼうふうつうしょうさん)
構成生薬 滑石 5, 石膏 3, 黄芩 2.5, 桔梗 2.5, 甘草 2, 荊芥 2, 山梔子 2, 白朮 2, 芒硝 1.2, 芍薬 1.2, 川芎 1.2, 当帰 1.2, 薄荷 1.2, 麻黄 1.2, 連翹 1.2, 防風 1.2, 生姜 1, 大黄 2
原典 黄帝素問宣明論
化合物名 Ephedrine+Pseudoephedrine,Genipingentiobioside,Geniposide,Apioliquiritin,Liquiritin,Pentagalloylgulucose,Sennoside B,Baicalin,Dihydroxybaicalein-7-O-glucuronide,Oroxylin A-7-O-glucoside,Wogonoside,Licorice-saponin E2,Glycyrrhizin,Sucrose,Tryptophane,Raffinose,Ephedrine,Proline
分析条件  
備考  

【 EXP037001 】
Peak No.12345678910111213
Compound nameGeniposide   SucroseTryptophaneRaffinoseEphedrineProline    
tR(min)3.194.686.419.6710.7715.3115.9117.1418.6819.7120.0120.6123.57
UV/Vis max (nm) 1     247200      
UV/Vis max (nm) 2             
UV/Vis max (nm) 3             
UV/Vis max (nm) 4             
UV/Vis max (nm) 5             
HR-MS 1 (base peak, m/z)406.16834461.10482469.16727360.1477360.14783205.09579522.19932166.1215116.06964130.09655138.05394144.10089122.92352
HR-MS 1 intensity100100100100100100100100100100100100100
HR-MS 2 (2nd)461.10498447.08935447.08935447.08915447.0893522.19937182.07989148.11106147.07532112.08608130.0965202.17884206.88451
HR-MS 2 intensity63.6564.3876.1862.0136.8489.3996.6814.4411.8826.724227.7988
HR-MS 3 (3rd)447.08947549.15666453.17256244.09117325.11095840.43202274.09032180.1371270.0645116.06973118.08531118.08532290.84536
HR-MS 3 intensity56.5946.2424.527.5716.168.0595.8911.159.5815.533.8221.2878.09
HR-MS2 for base peak, 1149.04843285.13647235.02771163.08356163.07242 163.03658      
HR-MS2 for base peak, 2177.04248 259.05295180.06439180.08888 289.01617      
HR-MS2 for base peak, 3181.22397 261.14401198.043198.11691 324.35132      
HR-MS2 for base peak, 4191.05243 289.13336276.82874258.82321 325.06116      
HR-MS2 for base peak, 5208.97845 290.13641288.8512288.85425 342.14355      
HR-MS2 for base peak, 6226.9707 291.11288307.04535306.92188 342.7832      
HR-MS2 for base peak, 7370.51303 307.0889324.25638324.25873 485.42535      
HR-MS2 for base peak, 8371.15091 308.09283324.95352325.02045 486.68903      
HR-MS2 for base peak, 9387.28445 397.12527342.03592342.15366 503.53247      
HR-MS2 for base peak, 10388.25552 451.04156342.74527342.89685 504.6095      
HR-MS2 for 2nd MS, 1285.07559271.00815271.04587271.03424271.02896288.85345       
HR-MS2 for 2nd MS, 2     300.09857       
HR-MS2 for 2nd MS, 3     324.46741       
HR-MS2 for 2nd MS, 4     325.08496       
HR-MS2 for 2nd MS, 5     342.81372       
HR-MS2 for 2nd MS, 6     360.1629       
HR-MS2 for 2nd MS, 7     437.47437       
HR-MS2 for 2nd MS, 8     476.11371       
HR-MS2 for 2nd MS, 9     486.39764       
HR-MS2 for 2nd MS, 10     504.22302