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防風通聖散エキス/ODS
防風通聖散エキス/ODS
【HILIC】

漢方方剤名 防風通聖散 (ぼうふうつうしょうさん)
構成生薬 滑石 5, 石膏 3, 黄芩 2.5, 桔梗 2.5, 甘草 2, 荊芥 2, 山梔子 2, 白朮 2, 芒硝 1.2, 芍薬 1.2, 川芎 1.2, 当帰 1.2, 薄荷 1.2, 麻黄 1.2, 連翹 1.2, 防風 1.2, 生姜 1, 大黄 2
原典 黄帝素問宣明論
化合物名 Ephedrine+Pseudoephedrine,Genipingentiobioside,Geniposide,Apioliquiritin,Liquiritin,Pentagalloylgulucose,Sennoside B,Baicalin,Dihydroxybaicalein-7-O-glucuronide,Oroxylin A-7-O-glucoside,Wogonoside,Licorice-saponin E2,Glycyrrhizin,Sucrose,Tryptophane,Raffinose,Ephedrine,Proline
分析条件  
備考  

【 EXP037001 】
Peak No.12345678910111213
Compound nameEphedrine+PseudoephedrineGenipingentiobiosideGeniposideApioliquiritinLiquiritinPentagalloylgulucoseSennoside BBaicalinDihydroxybaicalein-7-O-glucuronideOroxylin A-7-O-glucosideWogonosideLicorice-saponin E2Glycyrrhizin
tR(min)2.525.335.648.438.598.819.5911.5312.6612.9613.616.1217.08
UV/Vis max (nm) 1 226238219219226221275222217273223226
UV/Vis max (nm) 2 276 275276262299315279272340  
UV/Vis max (nm) 3 313 309311411   311   
UV/Vis max (nm) 4             
UV/Vis max (nm) 5             
HR-MS 1 (base peak, m/z)166.122291.08553209.0801257.08023257.0801315.07027543.14853447.0913447.09134461.1069461.1068451.31962453.33494
HR-MS 1 intensity100100100100100100100100100100100100100
HR-MS 2 (2nd)148.11142292.08884777.27938315.07035549.15889316.07367303.04922448.09462477.10155462.11026462.11017821.39361823.409
HR-MS 2 intensity22.1316.2625.2324.4832.6113.8155.5723.2363.4924.4424.333.8499.45
HR-MS 3 (3rd)149.02268149.0227177.05396258.08358307.11675549.15918315.07037 448.09465  452.32298824.41222
HR-MS 3 intensity12.9913.9313.9115.8721.0713.6929.45 22.66  31.6944.67
HR-MS2 for base peak, 1 122.98634   127.11162171.03415270.95251270.92355284.98077284.94058145.13147189.06081
HR-MS2 for base peak, 2 126.99186   152.93506252.99139 284.98578  285.13629241.14105
HR-MS2 for base peak, 3 138.92673   170.89304270.96869    297.0296267.11237
HR-MS2 for base peak, 4 147.02838   233.03683284.94803    301.02643285.13641
HR-MS2 for base peak, 5 150.96521   236.86105294.95953    311.11444299.09259
HR-MS2 for base peak, 6 164.99338   250.96466296.91534    341.13898311.09769
HR-MS2 for base peak, 7 169.05759   260.88336314.95178    355.04892330.95441
HR-MS2 for base peak, 8 181.09186   266.99149319.0249    405.064389.09717
HR-MS2 for base peak, 9 248.9751   278.82001336.89282    407.00269407.16525
HR-MS2 for base peak, 10 272.95779   296.849524.81213    433.04623435.03952
HR-MS2 for 2nd MS, 1 123.02547226.94562126.95935410.97491152.96497148.97617271.02054300.91956285.00793284.97333311.2027393.04175
HR-MS2 for 2nd MS, 2 124.00229324.74341144.94383428.8996153.93185152.96933271.88794 285.93646285.97113352.77112407.14313
HR-MS2 for 2nd MS, 3 138.91995352.7561152.95828440.84558171.0033165.04601    433.11859425.34247
HR-MS2 for 2nd MS, 4 140.01883370.93262170.98068452.87756171.93506206.92236    451.07629453.21216
HR-MS2 for 2nd MS, 5 148.11404388.01459213.02786464.88727233.99582214.86743    469.15265471.17792
HR-MS2 for 2nd MS, 6 150.90338388.84418232.93784476.93109238.00705228.9433    627.13721646.50568
HR-MS2 for 2nd MS, 7 152.05597532.57587236.80121482.90686261.9162234.98834    644.89716647.14899
HR-MS2 for 2nd MS, 8 164.97633550.45367260.90417494.94427267.88342247.00284    801.83167 
HR-MS2 for 2nd MS, 9 166.02682596.44348278.98917512.87946279.85217256.96875    802.70111 
HR-MS2 for 2nd MS, 10 273.88931614.17419296.90848530.87299297.81613284.91092