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遠志-2エキス/ODS
遠志-2エキス/ODS
【HILIC】

生薬名 遠志 (おんじ)
基原 Polygala tenuifolia Willdenow, イトヒメハギ (ヒメハギ科 Polygalaceae)
化合物名 Polygalaxanthone III,Sucrose,Asparagine
分析条件  
備考  

【 EXC008002 】
Peak No.1234567891011121314151617181920
Compound name      Polygalaxanthone III             
tR(min)3.273.424.664.975.166.257.47.647.879.7710.0410.91212.5712.9513.1313.7114.4316.7117.12
UV/Vis max (nm) 1208200222219229222229222258237222233225229224228228224224225
UV/Vis max (nm) 2265265323327329326262309318329326253301317300315317316312311
UV/Vis max (nm) 3      314 361  310        
UV/Vis max (nm) 4      375             
UV/Vis max (nm) 5                    
HR-MS 1 (base peak, m/z)287.16728206.14086257.15653339.10663369.11713219.14855539.13783569.14833369.11701369.11701339.10653383.13247397.12707413.12189239.09057413.12182413.12193413.12185203.06952367.1376
HR-MS 1 intensity100100100100100100100100100100100100100100100100100100100100
HR-MS 2 (2nd)287.66883206.64242257.65802257.1565370.12048387.12767540.14135570.15179370.12037387.12748369.11702384.13581413.12189414.12526397.12696383.13254414.12529414.12522501.31961501.31948
HR-MS 2 intensity33.4326.0331.826.4618.4750.6125.4226.5818.3730.673.1619.8483.6124.0968.3279.9524.1823.9489.0797.19
HR-MS 3 (3rd)156.06506197.62767338.18272340.10998267.08562219.6502412.25831354.21671362.06354370.12038387.12753283.08035383.13266501.31953383.13253414.12518443.13239443.13227307.11666307.11659
HR-MS 3 intensity22.7620.311.4917.1717.8129.511.3210.8611.3218.7362.317.3757.8510.4567.6824.385.756.6674.172.47
HR-MS2 for base peak, 1   177.2303207.24182 287.07117317.02155175.1748175.22272177.23831221.1743127.2915147.24623 147.23277147.22641147.28345 221.15881
HR-MS2 for base peak, 2      311.14545341.04834207.13666207.15341  131.30827201.21924 200.79164200.87877200.98544 348.9863
HR-MS2 for base peak, 3      341.01343371.03711    149.30061395.08673 229.13864394.45871394.99149  
HR-MS2 for base peak, 4      353.0661383.07495    200.97449  395.03922395.13361   
HR-MS2 for base peak, 5      388.97192401.06921    213.24011       
HR-MS2 for base peak, 6      406.8996418.97229    226.02734       
HR-MS2 for base peak, 7       436.92413    257.24542       
HR-MS2 for base peak, 8       460.96283    360.77325       
HR-MS2 for base peak, 9       551.05768    378.22473       
HR-MS2 for base peak, 10            379.02588       
HR-MS2 for 2nd MS, 1    175.2122175.08209287.03998317.07086175.19147207.14626175.21887221.2287147.28067147.26637127.33755221.21559147.27606147.25273391.28506355.32932
HR-MS2 for 2nd MS, 2    207.19205207.22984288.13669341.10699207.14381225.0437207.15291222.1758200.94711148.26898131.29979 148.2229148.25269409.24603391.33237
HR-MS2 for 2nd MS, 3    208.21283225.2196312.12714371.05719208.2446368.89999  394.93076201.00912149.23509 200.87009201.0347419.32111393.28506
HR-MS2 for 2nd MS, 4     367.93948342.11694383.0304     231.19388201.08612 229.21771229.23636436.66647409.27762
HR-MS2 for 2nd MS, 5     368.89371354.13654401.01599     273.00885213.15564 231.07101231.17072437.30499419.14261
HR-MS2 for 2nd MS, 6      389.0376419.07739     394.89456226.11502 273.07593273.12592447.28345437.18451
HR-MS2 for 2nd MS, 7      389.9751436.94244      231.10904 394.90512394.94086454.69653447.0896
HR-MS2 for 2nd MS, 8      406.96497437.99451      257.04175  395.9986455.30606455.22687
HR-MS2 for 2nd MS, 9      407.90765460.94806      360.75162   465.20224465.16592
HR-MS2 for 2nd MS, 10       550.95972      379.00046   483.01376483.10809