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麻黄-2エキス/ODS
麻黄-2エキス/ODS
【HILIC】

生薬名 麻黄 (まおう)
基原 Ephedra sinica Stapf (マオウ科 Ephedraceae)
化合物名 Norephedrine,Ephedrine,Methylehedrine,(+)-Catechin,Pseudoephedrine+Methylephedrine
分析条件  
備考  

【 EXC076002 】
Peak No.1234567891011121314
Compound name NorephedrineEphedrineMethylehedrine          
tR(min)1.652.152.373.043.494.675.455.96.336.947.238.3612.0914.04
UV/Vis max (nm) 1 200200200 216200219217217218217 221
UV/Vis max (nm) 2 228257273 265279265271256271270 277
UV/Vis max (nm) 3 256      330336334337  
UV/Vis max (nm) 4 318            
UV/Vis max (nm) 5              
HR-MS 1 (base peak, m/z)130.04909152.10608166.12169180.1373369.06936234.55029291.08526137.1318595.16302220.05943565.15277579.16798137.13168206.57349
HR-MS 1 intensity10010010010010055.9610075.94100100100100100100
HR-MS 2 (2nd)166.12167134.09567148.11119166.12175276.01543193.0851292.08861191.03436345.55786565.15257330.55278580.1713281.06929206.07505
HR-MS 2 intensity50.5787.7520.212.2843.952.7716.1275.2436.5317.1324.8426.5462.4754.94
HR-MS 3 (3rd)259.09114328.17383167.12499181.14064166.12185140.96103140.96103389.21557596.16619140.96097566.156337.56035276.0152 
HR-MS 3 intensity25.8327.510.8911.8835.1541.5811.4772.5121.6914.4624.0920.3334.23 
HR-MS2 for base peak, 1      123.26868 456.98596 409.0379313.04858  
HR-MS2 for base peak, 2      139.20404 474.93982 427.00018337.22058  
HR-MS2 for base peak, 3      147.29556 480.99976 445.08459367.09308  
HR-MS2 for base peak, 4      151.26715 498.99524 457.09436379.11542  
HR-MS2 for base peak, 5      165.22429 511.11572 469.03607397.17047  
HR-MS2 for base peak, 6      273.01733 522.99286 481.04694415.06714  
HR-MS2 for base peak, 7        529.00879 499.02667432.97223  
HR-MS2 for base peak, 8        541.02826 511.01117561.08954  
HR-MS2 for base peak, 9        558.96027 528.98016   
HR-MS2 for base peak, 10        576.91266 546.95398   
HR-MS2 for 2nd MS, 1      123.40369 264.94116409.0271264.92764313.16327  
HR-MS2 for 2nd MS, 2      124.30795 315.87897427.03174279.83221337.1153  
HR-MS2 for 2nd MS, 3      139.30971 324.85428445.04761300.82159367.0564  
HR-MS2 for 2nd MS, 4      140.2435 332.42679457.11902309.89685379.04272  
HR-MS2 for 2nd MS, 5      148.28023 333.56458475.03906310.74442397.08453  
HR-MS2 for 2nd MS, 6      151.21121  481.07788312.10611415.07623  
HR-MS2 for 2nd MS, 7      152.30301  499.08386317.548433.08008  
HR-MS2 for 2nd MS, 8      165.19647  511.04755318.25763434.05768  
HR-MS2 for 2nd MS, 9      166.24863  529.01111318.94257560.98444  
HR-MS2 for 2nd MS, 10      274.22293  546.98505321.30151